Nuclear Magnetic Resonance Spectroscopy

Nuclear Magnetic Resonance Spectroscopy
Author: Joseph B. Lambert
Publisher: John Wiley & Sons
Total Pages: 485
Release: 2019-01-04
Genre: Science
ISBN: 1119295238

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Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.

Principles of Nuclear Magnetic Resonance Microscopy

Principles of Nuclear Magnetic Resonance Microscopy
Author: Paul T. Callaghan
Publisher:
Total Pages: 520
Release: 1993
Genre: Science
ISBN: 9780198539971

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Although nuclear magnetic resonance is perhaps best known for its spectacular utility in medical tomography, its potential applicability to fields such as biology, materials science, and chemical physics is being increasingly recognized as laboratory NMR spectrometers are adapted to enable small scale imaging. This excellent introduction to the subject explores principles and common themes underlying two key variants of NMR microscopy, and provides many examples of their use. Methods discussed are not only important to fundamental biological and physical research, but have applications to a wide variety of industries, including those concerned with petrochemicals, polymers, biotechnology, food processing, and natural product processing. The wide range of scientists interested in NMR microscopy will want to own a copy of this book.

Principles of Nuclear Magnetic Resonance in One and Two Dimensions

Principles of Nuclear Magnetic Resonance in One and Two Dimensions
Author: Richard R. Ernst
Publisher:
Total Pages: 0
Release: 2023
Genre: Nuclear magnetic resonance spectroscopy
ISBN: 9781383028621

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Nuclear magnetic resonance spectroscopy is one of the most powerful and versatile techniques now available for the study of molecular structure and reaction mechanisms. Written by recognised experts in the field, this classic account of modern NMR spectroscopy was heralded on its first publication in 1987 as 'the lasting text of its age'. The text provides a thoroughly comprehensive review of modern NMR techniques and the underlying principles. It describes the study of solutions and solids using one- and two-dimensional spectroscpy, providing both a solid theoretical foundation and a description of practical procedures. The material is presented in an intuitive manner within a rigorous mathematical framework, and is extensively illustrated throughout.

Nuclear Magnetic Resonance Spectroscopy

Nuclear Magnetic Resonance Spectroscopy
Author: John Henry Nelson
Publisher:
Total Pages: 488
Release: 2003
Genre: Education
ISBN:

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This is the only how-to volume that investigates the spectroscopy of a variety of nuclides other than H andC in depth. It contains extensive reference material and numerous problems, most of which include real spectra. It is written to provide users with the knowledge necessary to choose the most appropriate experiment to obtain the best quality spectra with the ability to fully interpret the data. The book covers basic theory of NMR spectroscopy, spectrum measurement, the chemical shift and examples for selected nuclei, symmetry and NMR spectroscopy, spin-spin coupling and NMR spin systems, typical magnitude of selected coupling constants, nuclear spin relaxation, the nuclear overhauser effect, editing C NMR spectra, two-dimensional NMR spectroscopy, dynamic NMR spectroscopy, lanthanide shift reagents (LSR), NMR of solids. For NMR spectroscopists and analytical chemists.

Spin Dynamics

Spin Dynamics
Author: Malcolm H. Levitt
Publisher: John Wiley & Sons
Total Pages: 824
Release: 2013-05-20
Genre: Science
ISBN: 1118681843

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Spin Dynamics: Basics of Nuclear Magnetic Resonance, Second Edition is a comprehensive and modern introduction which focuses on those essential principles and concepts needed for a thorough understanding of the subject, rather than the practical aspects. The quantum theory of nuclear magnets is presented within a strong physical framework, supported by figures. The book assumes only a basic knowledge of complex numbers and matrices, and provides the reader with numerous worked examples and exercises to encourage understanding. With the explicit aim of carefully developing the subject from the beginning, the text starts with coverage of quarks and nucleons and progresses through to a detailed explanation of several important NMR experiments, including NMR imaging, COSY, NOESY and TROSY. Completely revised and updated, the Second Edition features new material on the properties and distributions of isotopes, chemical shift anisotropy and quadrupolar interactions, Pake patterns, spin echoes, slice selection in NMR imaging, and a complete new chapter on the NMR spectroscopy of quadrupolar nuclei. New appendices have been included on Euler angles, and coherence selection by field gradients. As in the first edition, all material is heavily supported by graphics, much of which is new to this edition. Written for undergraduates and postgraduate students taking a first course in NMR spectroscopy and for those needing an up-to-date account of the subject, this multi-disciplinary book will appeal to chemical, physical, material, life, medical, earth and environmental scientists. The detailed physical insights will also make the book of interest for experienced spectroscopists and NMR researchers. • An accessible and carefully written introduction, designed to help students to fully understand this complex and dynamic subject • Takes a multi-disciplinary approach, focusing on basic principles and concepts rather than the more practical aspects • Presents a strong pedagogical approach throughout, with emphasis placed on individual spins to aid understanding • Includes numerous worked examples, problems, further reading and additional notes Praise from the reviews of the First Edition: "This is an excellent book... that many teachers of NMR spectroscopy will cherish... It deserves to be a ‘classic’ among NMR spectroscopy texts." NMR IN BIOMEDICINE "I strongly recommend this book to everyone...it is probably the best modern comprehensive description of the subject." ANGEWANDTE CHEMIE, INTERNATIONAL EDITION

Nuclear Magnetic Resonance of Liquid Crystals

Nuclear Magnetic Resonance of Liquid Crystals
Author: Ronald Y. Dong
Publisher: Springer Science & Business Media
Total Pages: 268
Release: 2012-12-06
Genre: Science
ISBN: 1468402080

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Liquid crystals have become ubiquitous in the displays for electronic devices, ranging from wrist watches to laptop computers. Nuclear magnetic resonance is one of the important mechanisms for determining their structures tures and properties. This book covers NMR techniques used in studying liquid crystals and present up to date results from such studies. Ronald Dong has worked on NMR in liquid crystals for much of his professional career. Topics covered include: Nuclear spin dynamics, orientational order, molecular field theories of liquid-crystal molecules, nuclear spin relaxation, spin relaxation, rotational and translational dynamics, internal dynamics of liquid-crystal molecules, NMR in liquid crystals; an appendix covers rotations, Euler angles and Wigner rotation matrices.

Nuclear Magnetic Resonance

Nuclear Magnetic Resonance
Author: P. J. Hore
Publisher: Oxford University Press, USA
Total Pages: 121
Release: 2015
Genre: Science
ISBN: 0198703414

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Although the practice of NMR spectroscopy has changed hugely over the last 20 years, the physical principles of liquid-state NMR, with which this book is concerned, remain essentially the same. The origins of chemical shifts, spin-spin couplings, chemical exchange, and spin relaxation, and their effects on the appearance of NMR spectra, were all already pretty well understood by 1995, at least at the level of most undergraduate chemistry courses. As a consequence, the ground covered by this second edition does not differ greatly from the first. The most significant additions, aimed at making the coverage of experimental techniques a little more contemporary, are sections on INEPT, HSQC, and three-dimensional NMR.

Nuclear Magnetic Resonance Spectroscopy of Boron Compounds

Nuclear Magnetic Resonance Spectroscopy of Boron Compounds
Author: Heinrich Nöth
Publisher: Springer Science & Business Media
Total Pages: 474
Release: 2012-12-06
Genre: Science
ISBN: 3642667570

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The revolutionary impetus of the NMR methods in organic chemistry has parallels in the field of boron chemistry. lIB NMR spectroscopy provided a basis for the elucida tion of structures and reactions of the boron hydrides. However, although many studies have been carried out with the higher boranes, carboranes, metalloboranes, etc. , and although certain patterns have emerged, the correlation between the observed chemical shift and the assigned structural unit is still not fully understood. Therefore, predictions in this area are still rather limited, and semiquantitative interpretations are not yet pos sible. Several years ago Eaton and Lipscomb sUpImarized the status in this field in their book "NMR Studies of Boron Hydrides and Related Compounds" and a plethora of new data has accumulated since then. The book also contained material on simple bo rane derivatives, but they were not discussed in any detail. On the other hand many systematic studies, both synthetic and spectroscopic, have been conducted on these simple boron materials in the last decade. Thus a large amount of NMR information is available, not only on lIB but also on 1 H, 1 3 C, and 14 N. However, this information is widely scattered in the literature, and often the data are not discussed at all. It see med appropriate, therefore, to collect these data and to present them in one volume.

Nuclear Magnetic Resonance and Relaxation

Nuclear Magnetic Resonance and Relaxation
Author: B. P. Cowan
Publisher: Cambridge University Press
Total Pages: 462
Release: 1997-04-17
Genre: Science
ISBN: 0521303931

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Advanced text on nuclear magnetic resonance.

Nuclear Magnetic Resonance

Nuclear Magnetic Resonance
Author: Krystyna Kamienska-Trela
Publisher: Royal Society of Chemistry
Total Pages: 553
Release: 2011
Genre: Reference
ISBN: 1849731470

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Each volume of "Nuclear Magnetic Resonance" comprises a combination of annual and biennial reports which together provide comprehensive coverage of the literature on this topic.