Mössbauer Spectroscopy and Transition Metal Chemistry

Mössbauer Spectroscopy and Transition Metal Chemistry
Author: P. Gütlich
Publisher: Springer Science & Business Media
Total Pages: 292
Release: 2013-11-11
Genre: Science
ISBN: 3662125455
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Two decades have passed since the original discovery of recoilless nuclear gamma resonance by Rudolf Mossbauer; the spectroscopic method based on this resonance effect - referred to as Mossbauer spectroscopy - has developed into a powerful tool in solid-state research. The users are chemists, physicists, biologists, geologists, and scientists from other disciplines, and the spectrum of problems amenable to this method has become extraordinarily broad. In the present volume we have confined ourselves to applications of Mossbauer spectroscopy to the area of transition elements. We hope that the book will be useful not only to non-Mossbauer special ists with problem-Oriented activities in the chemistry and physics of transition elements, but also to those actively working in the field of Mossbauer spectroscopy on systems (compounds as well as alloys) of transition elements. The first five chapters are directed to introducing the reader who is not familiar with the technique to the principles of the recoilless nuclear resonance effect, the hyperfme interactions between nuclei and electronic properties such as electric and magnetic fields, some essential aspects about measurements, and the evaluation of Moss bauer spectra. Chapter 6 deals with the interpretation of Mossbauer parameters of iron compounds. Here we have placed emphasis on the information about the electronic structure, in correlation with quantum chemical methods, because of its importance for chemical bonding and magnetic properties.

Mössbauer Spectroscopy and Transition Metal Chemistry

Mössbauer Spectroscopy and Transition Metal Chemistry
Author: Philipp Gütlich
Publisher: Springer
Total Pages: 569
Release: 2011-01-17
Genre: Science
ISBN: 9783540884279
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concentrates on teaching techniques using as much theory as needed. application of the techniques to many problems of materials characterization. Mössbauer spectroscopy is a profound analytical method which has nevertheless continued to develop. The authors now present a state-of-the art book which consists of two parts. The first part details the fundamentals of Mössbauer spectroscopy and is based on a book published in 1978 in the Springer series 'Inorganic Chemistry Concepts' by P. Gütlich, R. Link and A.X. Trautwein. The second part covers useful practical aspects of measurements, and the application of the techniques to many problems of materials characterization. The update includes the use of synchroton radiation and many instructive and illustrative examples in fields such as solid state chemistry, biology and physics, materials and the geosciences, as well as industrial applications. Special chapters on magnetic relaxation phenomena (S. Morup) and computation of hyperfine interaction parameters (F. Neese) are also included. The book concentrates on teaching the technique using theory as much as needed and as little as possible. The reader will learn the fundamentals of the technique and how to apply it to many problems of materials characterization. Transition metal chemistry, studied on the basis of the most widely used Mössbauer isotopes, will be in the foreground.

Mössbauer Spectroscopy Applied to Magnetism and Materials Science

Mössbauer Spectroscopy Applied to Magnetism and Materials Science
Author: G.J Long
Publisher: Springer Science & Business Media
Total Pages: 370
Release: 2013-06-29
Genre: Science
ISBN: 1489917632
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This book represents Volume 2 in a series on the use of Mossbauer spectroscopy in the study of magnetism and materials. However, the perceptive reader will notice some differences from Volume 1. Specifically, in order to market the book at a more affordable price for most universities and research laboratories, the book has been prepared in camera ready format The editors and the authors agreed to do this because there is a demand for such a book in the Mossbauer community. This format has placed an extra burden on the editors and the authors and we hope we have overcome all the difficulties generated by the transfer of files between different computers. In order to make the book more attractive to materials scientists who are not experts in Mossbauer spectroscopy, this volume is particularly oriented towards the study of materials by Mossbauer spectroscopy and related complementary techniques, such as neutron scattering and a variety of surface scattering techniques. The authors of this volume can be proud of the high quality professional effort they have devoted to clearly presenting their specific topics. As a result we very much enjoyed working with the authors on this volume. We hope that their effort will help to educate the next generation of Mossbauer effect spectroscopists, a generation which will face the challenge of maintaining equally high scientific and professional standards in their research work.

Mössbauer Spectroscopy

Mössbauer Spectroscopy
Author: Virender K. Sharma
Publisher: John Wiley & Sons
Total Pages: 1018
Release: 2013-08-13
Genre: Science
ISBN: 1118771974
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Providing a modern update of the field, Mossbauer Spectroscopy focuses on applications across a broad range of fields, including analysis of inorganic elements, nanoparticles, metalloenzymyes, biomolecules (including proteins), glass, coal, and iron. Ideal for a broad range of scientists, this one-stop reference presents advances gained in the field over past two decades, including a detailed theoretical description of Mossbauer spectroscopy, an extensive treatment of Mossbauer spectroscopy in applied areas, and challenges and future opportunities for the further development of this technique.

Mössbauer Spectroscopy Applied to Inorganic Chemistry

Mössbauer Spectroscopy Applied to Inorganic Chemistry
Author: G.J Long
Publisher: Springer Science & Business Media
Total Pages: 677
Release: 2013-11-11
Genre: Science
ISBN: 148990462X
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When presented with a new compound or material, the inorganic chemist will usually have several questions in mind about its composition and structure. Although a simple elemental analysis may answer many questions about its composition, the chemist will still have questions about its structure, and, ifthe material contains a metal atom, he will often want to know its oxidation state, coordination number and geometry. Further, at an increasingly frequent rate, the chemist may need details of the spin state, magnetic and perhaps dynamic properties of the material. If the investigator is fortunate, the material or compound may contain an ele ment such as iron, tin, antimony, iodine, gold, or one of several of the rare earth metals which are amenable to study by the Mossbauer effect. Often the Mossbauer effect can, sometimes with quite simple experiments, provide the answers to all of these questions. The goal of this book is to illustrate the effectiveness of the Mossbauer effect in providing the answers to the many questions that arise in char acterizing new materials and, indeed, in studying known materials in more detail. Several chapters introduce the effect to the novice and provide details about the various hyperfine interactions that are the "bread and butter" of the Mossbauer spectroscopist. Three chapters deal specifically with the experimental aspects of the technique and the increasing impor tance of sophisticated computer analysis of the resulting data.

Chemical Mössbauer Spectroscopy

Chemical Mössbauer Spectroscopy
Author: Rolfe Herber
Publisher: Springer
Total Pages: 400
Release: 1984
Genre: Gardening
ISBN:
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The past twenty five years - roughly the period from 1960 to 1985 - have been by all measures among the most exciting and challenging times of our science. The increasing sensitivity of chemical instrumentation, the introduction of the routine use of computers for data reduction and of microprocessors for instrumental control, the wide-spread utilization of lasers, and the disappearance of traditional disciplinary boundaries between scientific fields are but a few of the examples one could cite to support the introductory contention. Almost all of these developments have had their impact on the development of Mossbauer Effect Spectroscopy into a technique par excellence for the elucidation of problems in all areas of chemistry and its associated sister sciences. Indeed, because this spectroscopy is based on fundamental phenomena in nuclear physics, is described in terms of the theory of the solid state and structural chemistry, is useful in the understanding of chemical reactivity and biological phenomena, and can serve to supplement information developed by many other experimental techniques, it has provided an unparalleled opportunity for the exchange of ideas among practitioners of a very wide variety of subfields of the physical and biological sciences. The present collection of contributions is the direct result of such an interaction.

Perspectives in Mössbauer Spectroscopy

Perspectives in Mössbauer Spectroscopy
Author: S. Cohen
Publisher: Springer Science & Business Media
Total Pages: 258
Release: 2012-12-06
Genre: Science
ISBN: 1461586879
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This book is for the most part made up of the invited papers presented at the International Conference on Applica tions of the Kdssbauer effect, held at Aye1eth Hashahar, Israel, in August 1972. The purpose of the conference was to review perspec tives in MHssbauer spectroscopy from the point of view of applications in various fields of science - mainly physics, chemistry, and biology. It was hoped that the bringing together of scientists who work in different disciplines but use a common tool would encourage interdisciplinary re search and widen the horizon of the individual researcher. Both these features have been an important and unique characteristic of Kdssbauer research in the past decade. Accordingly, the main papers were presented in the following areas: magnetic properties of solids, applications to in organic chemistry, biochemical studies, amorphous systems, metal alloys, advances in high-resolution studies, and the new techniques for studying recoil-free spectra from isolated atoms in inert materials. A special panel discussion was devoted to the subject of phase transitions. Recent years have witnessed a rapid growth in the use of X-ray photoelec tron spectroscopy for the study of the physics and chemistry of solids. A report on this area of research and its rela tion to Kdssbauer studies has been included.

Mossbauer Spectroscopy

Mossbauer Spectroscopy
Author: Yann Garcia
Publisher: John Wiley & Sons
Total Pages: 342
Release: 2023-10-30
Genre: Science
ISBN: 3527346910
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Mössbauer Spectroscopy Unique and comprehensive overview of versatile applications of Mössbauer spectroscopy in chemistry and material sciences Mössbauer Spectroscopy provides a comprehensive overview of relevant applications of this physical analysis method in chemistry and material sciences. The book shows the versatility of Mössbauer spectroscopy in finding useful information on electronic structure, structural insights, and solid-state effects of chemical systems. A wide range of chemical applications and applied concepts are covered as well as numerous examples, selected from recent literature. To aid in reader comprehension and accessibility, contents are well-structured and divided in different sections covering energy, catalysis, coordination chemistry, spin crossover, sensing, photomagnetism. Edited by prominent scientists in the field and authored by a group of international experts, Mössbauer Spectroscopy covers sample topics such as: Li-ion batteries, catalysts, fuel cells, Fe based silicides and iron phosphates containing minerals Gold clusters and gold mixed valence complexes Molecule based magnets, photoswitchable spin crossover coordination polymers and molecular sensors for meat freshness control With comprehensive coverage of the developments in the technique, Mössbauer Spectroscopy is a beneficial resource for researchers, professionals, and academics in chemistry related fields, such as material science, sustainable environment, and molecular electronics. It can be used by newcomers as well as for educational purposes at the master and PhD levels.

An Introduction to Mössbauer Spectroscopy

An Introduction to Mössbauer Spectroscopy
Author: Leopold May
Publisher: Springer Science & Business Media
Total Pages: 213
Release: 2012-12-06
Genre: Science
ISBN: 1468489119
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The initial impetus for this text occurred when we were searching for a single book that could be recommended to the attendees at the Mossbauer Spectroscopy Institute at The Catholic University of America. This Institute is an introductory course on the theory and interpretation of Mossbauer spectroscopy for workers in industrial, academic, and government labora tories. None of the books available adequately covered the breadth and scope of the lectures in the Institute. A list of these books and review articles is included in Appendix C. To meet our needs, we undertook the creation of this text. The chapters are based upon the lectures given at the various Institutes from 1967 to 1969. Most of the lectures were recorded and transcripts sent to the lecturers, who then prepared the manuscripts, using the transcripts as a guide so as to retain the style developed during the lecture. Each chapter is written in the style of the authors. As the editor, my main task was to main tain uniformity of format and nomenclature. A list of nomenclature used in this volume is reproduced in Appendix A. We hope that this list will be used particularly by new investigators and teachers of Mossbauer spectroscopy so that future literature will employ a uniform system.