Polymer Characterization by Liquid Chromatography

Polymer Characterization by Liquid Chromatography
Author: G. Glöckner
Publisher: Elsevier
Total Pages: 589
Release: 1987-02-01
Genre: Science
ISBN: 0080858376

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The main subject of this book is the characterization of plastics. To a high degree the properties of these polymers depend on the distribution of the molar mass and of other structural features, and small deviations frequently have a great effect. Therefore the characterization of polymers cannot be restricted to the determination of mean values but must yield information on these distributions. Using classical methods, the analytical fractionation of polymer homologues and structurally isomeric polymers is extremely time-consuming. Therefore, efficient chromatographic techniques are being increasingly employed in modern polymer characterization. In the first place, high-performance liquid chromatography is applied, in the form of size exclusion chromatography. It is also possible, however, to use other separation modes. More space is devoted to these other possibilities in this volume than is merited by their current range of applications, as the author believes that many separation problems will be solved by separation techniques of the non-exclusion type. Nevertheless, much emphasis is placed on size exclusion chromatography. Not only because of its current wide range of applications, but also because its relative importance, as a complement to other chromatographic techniques may even increase in the forthcoming years. This book is the first to cover all phenomena related to the above considerations. Starting with an introduction to basic liquid chromatography and to polymer science, it deals with the adsorption behaviour of polymers, with gradient techniques, with the kinetic band broadening in liquid chromatography, with instrumental features and packing materials. The book consists of four balanced sections and related information from about 1800 references is compiled in the tables. Some 250 figures and 30 tables will help give the reader a clear insight of the topics discussed. The book is aimed at helping the analyst or polymer chemist who is looking for information about chromatographic methods for the characterization of polymers.

Molecular Characterization of Polymers

Molecular Characterization of Polymers
Author: Muhammad Imran Malik
Publisher: Elsevier
Total Pages: 670
Release: 2021-03-09
Genre: Technology & Engineering
ISBN: 012822598X

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Molecular Characterization of Polymers presents a range of advanced and cutting-edge methods for the characterization of polymers at the molecular level, guiding the reader through theory, fundamentals, instrumentation, and applications, and supporting the end goal of efficient material selection and improved material performance. Each chapter focuses on a specific technique or family of techniques, including the different areas of chromatography, field flow fractionation, long chain branching, static and dynamic light scattering, mass spectrometry, NMR, X-Ray and neutron scattering, polymer dilute solution viscometry, microscopy, and vibrational spectroscopy. In each case, in-depth coverage explains how to successfully implement and utilize the technique. This practical resource is highly valuable to researchers and advanced students in polymer science, materials science, and engineering, and to those from other disciplines and industries who are unfamiliar with polymer characterization techniques. Introduces a range of advanced characterization methods, covering aspects such as molecular weight, polydispersity, branching, composition, and tacticity Enables the reader to understand and to compare the available technique, and implement the selected technique(s), with a view to improving properties of the polymeric material Establishes a strong link between basic principles, characterization techniques, and real-life applications

HPLC of Polymers

HPLC of Polymers
Author: Harald Pasch
Publisher: Springer Science & Business Media
Total Pages: 234
Release: 2012-12-06
Genre: Technology & Engineering
ISBN: 3642582656

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Polymers are mainly characterized by molar mass, chemical composition, functionality and architecture. The determination of the complex structure of polymers by chromatographic and spectroscopic methods is one of the major concerns of polymer analysis and characterization. This lab manual describes the experimental approach to the chromatographic analysis of polymers. Different chromatographic methods, their theoretical background, equipment, experimental procedures and applications are discussed. The book will enable polymer chemists, physicists and material scientists as well as students of macromolecular and analytical science to optimize chromatographic conditions for a specific separation problem. Special emphasis is given to the description of applications for homo- and copolymers and polymer blends.

Modern Methods of Polymer Characterization

Modern Methods of Polymer Characterization
Author: Howard G. Barth
Publisher: John Wiley & Sons
Total Pages: 582
Release: 1991-09-03
Genre: Science
ISBN: 9780471828143

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Presents the methods used for characterization of polymers. In addition to theory and basic principles, the instrumentation and apparatus necessary for methods used to study the kinetic and thermodynamic interactions of a polymer with its environment are covered in detail. Some of the methods examined include polymer separations and characterization by size exclusion and high performance chromatography, inverse gas chromatography, osmometry, viscometry, ultracentrifugation, light scattering and spectroscopy.

Characterization and Analysis of Polymers by Gas Chromatography

Characterization and Analysis of Polymers by Gas Chromatography
Author: Malcolm P. Stevens
Publisher: Marcel Dekker
Total Pages: 224
Release: 1969
Genre: Science
ISBN:

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Written primarily to help the polymer chemist in streamlining his analytical techniques.

Chromatographic Characterization of Polymers

Chromatographic Characterization of Polymers
Author: Theodore Provder
Publisher:
Total Pages: 322
Release: 1995
Genre: Language Arts & Disciplines
ISBN:

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Presents an overview of the recent developments in the use of hyphenated multidimensional separation and detection techniques for the characterization of polymeric materials. Reports on successful multidimensional chromatographic methods and multiple detector systems. Includes an analysis of compositional heterogeneity in copolymers and blends.

Characterization and Analysis of Polymers

Characterization and Analysis of Polymers
Author: Wiley
Publisher: John Wiley & Sons
Total Pages: 987
Release: 2008-02-08
Genre: Technology & Engineering
ISBN: 0470233001

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Based on Wiley's renowned Encyclopedia of Polymer Science and Technology, this book provides coverage of key methods of characterization of the physical and chemical properties of polymers, including atomic force microscopy, chromatographic methods, laser light scattering, nuclear magnetic resonance, and thermal analysis, among others. Written by prominent scholars from around the world, this reference presents over twenty-five self -contained articles on the most used analytical techniques currently practiced in polymer science.

Analytical Methods for Polymer Characterization

Analytical Methods for Polymer Characterization
Author: Rui Yang
Publisher: CRC Press
Total Pages: 296
Release: 2018-01-09
Genre: Science
ISBN: 1351213148

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Analytical Methods for Polymer Characterization presents a collection of methods for polymer analysis. Topics include chromatographic methods (gas chromatography, inverse gas chromatography, and pyrolysis gas chromatography), mass spectrometry, spectroscopic methods (ultraviolet-visible spectroscopy, infrared spectroscopy, Raman spectroscopy, and nuclear magnetic resonance), thermal analysis (differential scanning calorimetry and thermogravimetry), microscopy methods (scanning electron microscopy, transmission electron microscopy, and atomic force microscopy), and x-ray diffraction. The author also discusses mechanical and dynamic mechanical properties.