Advanced Coal Liquefaction Research and Development Facility, Wilsonville, Alabama. Run 262 with Black Thunder Subbituminous Coal

Advanced Coal Liquefaction Research and Development Facility, Wilsonville, Alabama. Run 262 with Black Thunder Subbituminous Coal
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Total Pages: 208
Release: 1992
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This report presents the results of Run 262 performed at the Advanced Coal Liquefaction R & D Facility in Wilsonville, Alabama. The run started on July 10, 1991 and continued until September 30, 1991, operating in the Close-Coupled Integrated Two-Stage Liquefaction mode processing Black Thunder Mine subbituminous coal (Wyodak-Anderson seam from Wyoming Powder River Basin). A dispersed molybdenum catalyst was evaluated for its performance. The effect of the dispersed catalyst on eliminating solids buildup was also evaluated. Half volume reactors were used with supported Criterion 324 1/16'' catalyst in the second stage at a catalyst replacement rate of 3 lb/ton of MF coal. The hybrid dispersed plus supported catalyst system was tested for the effect of space velocity, second stage temperature, and molybdenum concentration. The supported catalyst was removed from the second stage for one test period to see the performance of slurry reactors. Iron oxide was used as slurry catalyst at a rate of 2 wt % MF coal throughout the run (dimethyl disulfide (DMDS) was used as the sulfiding agent). The close-coupled reactor unit was on-stream for 1271.2 hours for an on-stream factor of 89.8% and the ROSE-SR unit was on-feed for 1101.6 hours for an on-stream factor of 90.3% for the entire run.

Advanced Coal Liquefaction Research and Development Facility, Wilsonville, Alabama

Advanced Coal Liquefaction Research and Development Facility, Wilsonville, Alabama
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Publisher:
Total Pages: 208
Release: 1992
Genre:
ISBN:

Download Advanced Coal Liquefaction Research and Development Facility, Wilsonville, Alabama Book in PDF, Epub and Kindle

This report presents the results of Run 262 performed at the Advanced Coal Liquefaction R D Facility in Wilsonville, Alabama. The run started on July 10, 1991 and continued until September 30, 1991, operating in the Close-Coupled Integrated Two-Stage Liquefaction mode processing Black Thunder Mine subbituminous coal (Wyodak-Anderson seam from Wyoming Powder River Basin). A dispersed molybdenum catalyst was evaluated for its performance. The effect of the dispersed catalyst on eliminating solids buildup was also evaluated. Half volume reactors were used with supported Criterion 324 1/16'' catalyst in the second stage at a catalyst replacement rate of 3 lb/ton of MF coal. The hybrid dispersed plus supported catalyst system was tested for the effect of space velocity, second stage temperature, and molybdenum concentration. The supported catalyst was removed from the second stage for one test period to see the performance of slurry reactors. Iron oxide was used as slurry catalyst at a rate of 2 wt % MF coal throughout the run (dimethyl disulfide (DMDS) was used as the sulfiding agent). The close-coupled reactor unit was on-stream for 1271.2 hours for an on-stream factor of 89.8% and the ROSE-SR unit was on-feed for 1101.6 hours for an on-stream factor of 90.3% for the entire run.

Advanced Coal Liquefaction Research and Development Facility, Wilsonville, Alabama. Run 260 with Black Thunder Mine Subbituminous Coal

Advanced Coal Liquefaction Research and Development Facility, Wilsonville, Alabama. Run 260 with Black Thunder Mine Subbituminous Coal
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Total Pages: 210
Release: 1992
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This report presents the results of Run 260 performed at the Advanced Coal Liquefaction R & D Facility in Wilsonville. The run was started on July 17, 1990 and continued until November 14, 1990, operating in the Close-Coupled Integrated Two-Stage Liquefaction mode processing Black Thunder mine subbituminous coal (Wyodak-Anderson seam from Wyoming Powder River Basin). Both thermal/catalytic and catalytic/thermal tests were performed to determine the methods for reducing solids buildup in a subbituminous coal operation, and to improve product yields. A new, smaller interstage separator was tested to reduce solids buildup by increasing the slurry space velocity in the separator. In order to obtain improved coal and resid conversions (compared to Run 258) full-volume thermal reactor and 3/4-volume catalytic reactor were used. Shell 324 catalyst, 1/16 in. cylindrical extrudate, at a replacement rate of 3 lb/ton of MF coal was used in the catalytic stage. Iron oxide was used as slurry catalyst at a rate of 2 wt % MF coal throughout the run. (TNPS was the sulfiding agent.).

The Wilsonville Advanced Coal Liquefaction Research and Development Facility, Wilsonville, Alabama

The Wilsonville Advanced Coal Liquefaction Research and Development Facility, Wilsonville, Alabama
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Total Pages: 117
Release: 1990
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This reports presents the operating results for Run 252 at the Advanced Coal Liquefaction R D Facility in Wilsonville, Alabama. This run operated in the Close-Coupled Integrated Two-Stage Liquefaction mode (CC-ITSL) using Illinois No. 6 bituminous coal. The primary run objective was demonstration of unit and system operability in the CC-ITSL mode with catalytic-catalytic reactors and with ash recycle. Run 252 began on 26 November 1986 and continued through 3 February 1987. During this period 214.4 MF tons of Illinois No. 6 coal were fed in 1250 hours of operation. 3 refs., 29 figs., 18 tabs.

Advanced Coal Liquefaction Research and Development Facility, Wilsonville, Alabama. Run 261 with Illinois No. 6 Burning Star Mine Coal

Advanced Coal Liquefaction Research and Development Facility, Wilsonville, Alabama. Run 261 with Illinois No. 6 Burning Star Mine Coal
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Total Pages: 239
Release: 1992
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This report presents the results of Run 261 performed at the Advanced Coal Liquefaction R & D Facility in Wilsonville, Alabama. The run started on January 12, 1991 and continued until May 31, 1991, operating in the Close-Coupled Integrated Two-Stage Liquefaction mode processing Illinois No. 6 seam bituminous coal (from Burning star No. 2 mine). In the first part of Run 261, a new bimodal catalyst, EXP-AO-60, was tested for its performance and attrition characteristics in the catalytic/catalytic mode of the CC-ITSL process. The main objective of this part of the run was to obtain good process performance in the low/high temperature mode of operation along with well-defined distillation product end boiling points. In the second part of Run 261, Criterion (Shell) 324 catalyst was tested. The objective of this test was to evaluate the operational stability and catalyst and process performance while processing the high ash Illinois No. 6 coal. Increasing viscosity and preasphaltenes made it difficult to operate at conditions similar to EXP-AO-60 catalyst operation, especially at lower catalyst replacement rates.

Wilsonville Advanced Coal-Liquefaction Research and Development Facility, Wilsonville, Alabama. Topical Report No. 5. 6000 TPD SRC-I Demonstration Plant Support

Wilsonville Advanced Coal-Liquefaction Research and Development Facility, Wilsonville, Alabama. Topical Report No. 5. 6000 TPD SRC-I Demonstration Plant Support
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Release: 1983
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Initially, the Wilsonville facility consisted of a single stage (thermal) process, also known as the SRC-I process. The original plant has been expanded to become an advanced two-stage coal liquefaction facility. A Critical Solvent Deashing (CDS) unit was installed in 1978 and a second stage catalytic hydrogenation (HTR) unit was installed in 1981. The principal product of the first stage is a low sulfur solid fuel. The reaction product is deashed by the CSD unit using a proprietary process developed by the Kerr-McGee Corporation. The hydrotreater, or the second stage, was installed primarily for further enhancement of product properties, process flexibility, and overall hydrogen utilization efficiency. In the decoupled mode of operation, the HTR unit has no direct effect on the SRC unit. This operating mode is called the non-integrated two-stage liquefaction (NTSL) process. From 17 October 1981 to 14 October 1982, the Advanced Coal Liquefaction R and D Facility at Wilsonville, Alabama, was operated partly in support of the 6000 TPD-I demonstration plant design effort undertaken by ICRC. The ICRC support tests and operations performed were: Run 235 with Kentucky 9 (Fies) coal; Run 240 with Illinois 6 (Burning Star) coal; CSD unit second stage variability study; CSD unit continuous ash removal system study; SRC solidification test; wastewater sampling operation; and residual fuel oil blending operation.