Micro Reaction Technology in Organic Synthesis

Micro Reaction Technology in Organic Synthesis
Author: Charlotte Wiles
Publisher: CRC Press
Total Pages: 453
Release: 2016-04-19
Genre: Science
ISBN: 143982472X

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While continuous processes have found widespread application within chemical production, members of the research and development communities have historically favored the centuries old technique of iterative batch reactions. With the exception of combinatorial and microwave chemistry, little had been done to change the way that synthetic chemists c

Microreactors in Organic Synthesis and Catalysis

Microreactors in Organic Synthesis and Catalysis
Author: Thomas Wirth
Publisher: John Wiley & Sons
Total Pages: 297
Release: 2008-09-08
Genre: Science
ISBN: 3527622861

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This one-stop reference is the first book on this emerging and rapid developing field with a focus on synthesis and catalysis. As such, it covers all aspects from academia and industry in a clearly structured way. Leading experts provide the background information as an initial aid for newcomers to the field, while chapters on different reaction types and industrial applications make this an equally vital resource for specialists.

Microreaction Technology

Microreaction Technology
Author: M. Matlosz
Publisher: Springer Science & Business Media
Total Pages: 584
Release: 2012-12-06
Genre: Science
ISBN: 3642567630

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IMRET 5 featured more than 80 oral and poster communications, covering the entire interdisciplinary field from design, production, modeling and characterization of microreactor devices to application of microstructured systems for production, energy and transportation, including many analytical and biological applications. A particularly strong topic was the investigation of the potential of microstructuring of reactors and systems components for process intensification. Perspectives of combining local, in situ, data acquisition with appropriate microstructuring of actuators and components within chemical and biological devices were explored in order to enhance process performance and facilitate process control.

Chemical Micro Process Engineering

Chemical Micro Process Engineering
Author: Volker Hessel
Publisher: John Wiley & Sons
Total Pages: 720
Release: 2004-04-12
Genre: Science
ISBN: 9783527307418

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A MULTI-FACETED, HIERARCHIC ANALYSIS OF CHEMICAL MICRO PROCESS TECHNOLOGY Micro Reactor Differentiation and Process Intensification Consequences of Chemical Micro Processing Physical and Chemical Implications Impact on Chemical Engineering Impact on Process Engineering Impact on Process Results Impact on Society and Ecology Impact on Economy Application Fields and Markets of Micro Reactors MODELLING AND SIMULATION OF MICRO REACTORS Flow Phenomena on the Microscale Methods of Computational Fluid Dynamics Flow Distributions Heat Transfer Mass Transfer and Mixing Reaction Kinetics and Modelling Free Surface Flow Flow in Porous Media GAS-PHASE REACTIONS Catalyst Coatings in Micro Channels Micro Reactors for Gas-Phase Reactions Oxidations Hydrogenations Dehydrogenations Substitutions Eliminations Additions and Coupling Reactions LIQUID- AND LIQUID/LIQUID-PHASE REACTIONS Micro Reactors for Liquid-Phase and Liquid/Liquid-Phase Recations Aliphatic Nucleophilic and Electrophilic Substitution such as Esterification, Acylation of Amines, Thiocyanation, and much more Aromatic Electrophilic and Nucleophilic Substitution such as Nitrations, Amino-de-halogenations, Diazo Chemistry, and much more Metal-catalysed Aromatic Substitution such as Suzuki and Sonogashira Couplings, and more Free Radical Substitution such as Alkane Nitration Addition to Carbon-Carbon and Carbon-hetero Multiple Bonds such as the Michael Addition, the Diels-Alder-Reaction, the Aldol Reaction, and much more Oxidations and Reductions Eliminations and Rearrangements Inorganic Reactions such as the Belousov-Zhabotinskii-Reaction, Complex Formations, and much more GAS/LIQUID CONTACTING Micro Reactors for Gas/Liquid Contacting Aromatic Electrophilic Substitution such as Direct Fluorinations Free Radical Substitution such as Alkane Fluorinations and Chlorinations Addition to Carbon-Carbon and Carbon-hetero Multiple Bonds such as Nitro-group Hydrogenation, Cycloalkane Hydrogenation, and more Oxidations and Reductions such as Alcohol Oxidation, Photo Diels-Alder Reactions, and more Inorganic Reactions such as Sulfite Oxidation.

Chemical Micro Process Engineering

Chemical Micro Process Engineering
Author: Volker Hessel
Publisher: John Wiley & Sons
Total Pages: 681
Release: 2006-03-06
Genre: Science
ISBN: 3527606270

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Micro process engineering is approaching both academia and industry. With the provision of micro devices, systems and whole plants by commercial suppliers, one main barrier for using these units has been eliminated. This book focuses on processes and their plants rather than on devices: what is 'before', 'behind' and 'around' micro device fabrication - and gives a comprehensive and detailed overview on the micro-reactor plants and three topic-class applications which are mixing, fuel processing, and catalyst screening. Thus, the book reflects the current level of development from 'micro-reactor design' to 'micro-reactor process design'.

Microreactors in Organic Chemistry and Catalysis

Microreactors in Organic Chemistry and Catalysis
Author: Thomas Wirth
Publisher: John Wiley & Sons
Total Pages: 493
Release: 2013-02-22
Genre: Science
ISBN: 3527659749

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For the second edition of 'Microreactors in Organic Chemistry and Catalysis' all chapters have been revised and updated to reflect the latest developments in this rapidly developing field. This new edition has 60% more content, and it remains a comprehensive publication covering most aspects of the topic. The use of microreactors in homogeneous, heterogeneous as well as biphasic reactions is covered in the main part of the book, together with catalytic, bioorganic and automation approaches. The initial chapters also provide a solid physical chemistry background on fluidics in microdevices. Finally, a chapter on industrial applications and developments covers recent progress in process chemistry. An excellent reference for beginners and experts alike.

Microreaction Technology: Industrial Prospects

Microreaction Technology: Industrial Prospects
Author: W. Ehrfeld
Publisher: Springer Science & Business Media
Total Pages: 707
Release: 2012-12-06
Genre: Science
ISBN: 3642597386

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Miniaturization has cost and time-saving advantages for numerous applications in chemistry, pharmacy, medicine and biotechnology. Additionally, microreaction technology offers new solutions for the automobile industry and environmental technology, e.g. fuel cells, or mobile sensor systems for on-the-spot analysis. Therefore, the 3rd International Conference on Microreaction Technology - IMRET 3 is an important forum for creating awareness of the wide variety of the new trends in this up-and-coming discipline.

Chemical Micro Process Engineering

Chemical Micro Process Engineering
Author: Volker Hessel
Publisher: Wiley-VCH
Total Pages: 696
Release: 2005-04-15
Genre: Science
ISBN:

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Micro process engineering is approaching both academia and industry. With the provision of micro devices, systems and whole plants by commercial suppliers, one main barrier for using these units has been eliminated. This book focuses on processes and their plants rather than on devices: what is 'before', 'behind' and 'around' micro device fabrication - and gives a comprehensive and detailed overview on the micro-reactor plants and three topic-class applications which are mixing, fuel processing, and catalyst screening. Thus, the book reflects the current level of development from 'micro-reactor design' to 'micro-reactor process design'.

Microwaves in Organic Synthesis

Microwaves in Organic Synthesis
Author: André Loupy
Publisher: Wiley-VCH
Total Pages: 536
Release: 2002
Genre: Science
ISBN:

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If the source materials and products fail to withstand the usually long reaction times at high temperatures and decompose, the yield is normally reduced. Therefore, the demand for increasingly clean and efficient chemical syntheses is continuously becoming more urgent from both an economic and an environmental standpoint. So-called green technologies are looking for alternative ways to reduce such drastic prerequisites for reactions. It is against this background that microwave technology has developed all the more into a powerful alternative that can be applied to practically the whole spectrum of organic synthesis. This volume brings together the latest developments in this fascinating field, supplemented by numerous practical tips, and thus provides those working in both research and industry with an indispensable source of information.

Stereoselective Synthesis of Drugs and Natural Products

Stereoselective Synthesis of Drugs and Natural Products
Author: Vasyl Andrushko
Publisher: John Wiley & Sons
Total Pages: 1836
Release: 2013-08-16
Genre: Science
ISBN: 1118628330

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Brings together the best tested and proven stereoselective synthetic methods Both the chemical and pharmaceutical industries are increasingly dependent on stereoselective synthetic methods and strategies for the generation of new chiral drugs and natural products that offer specific 3-D structures. With the publication of Stereoselective Synthesis of Drugs and Natural Products, researchers can turn to this comprehensive two-volume work to guide them through all the core methods for the synthesis of chiral drugs and natural products. Stereoselective Synthesis of Drugs and Natural Products features contributions from an international team of synthetic chemists and pharmaceutical and natural product researchers. These authors have reviewed the tremendous body of literature in the field in order to compile a set of reliable, tested, and proven methods alongside step-by-step guidance. This practical resource not only explores synthetic methodology, but also reaction mechanisms and applications in medicinal chemistry and drug discovery. The publication begins with an introductory chapter covering general principles and methodologies, nomenclature, and strategies of stereoselective synthesis. Next, it is divided into three parts: Part One: General Methods and Strategies Part Two: Stereoselective Synthesis by Bond Formation including C-C bond formation C-H bond formation C-O bond formation C-N bond formation Other C-heteroatom formation and other bond formation Part Three: Methods of Analysis and Chiral Separation References in every chapter serve as a gateway to the literature in the field. With this publication as their guide, chemists involved in the stereoselective synthesis of drugs and natural products now have a single, expertly edited source for all the methods they need.